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1 article(s) from Leza, Nerea Jordana

Synthesis and anion recognition properties of shape-persistent binaphthyl-containing chiral macrocyclic amides

Marco Caricato,
Nerea Jordana Leza,
Claudia Gargiulli,
Giuseppe Gattuso,
Daniele Dondi and
Dario Pasini

Beilstein J. Org. Chem. 2012, 8, 967–976, doi:10.3762/bjoc.8.109

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Figure 1: Structure of the macrocycle (R,R)-1 (top), and synthetic strategies for the production of novel ami...

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Scheme 1: Reagents and conditions: (i) SOCl₂, CHCl₃ or (COCl)₂, DMF, CH₂Cl₂ then amine, Et₃N, CH₂Cl₂ or (ii) ...

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Scheme 2: Structure and synthesis of the macrocycles discussed in this paper.

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Figure 2: UV and CD (EtOH) spectra of macrocycles (R,R)-10, (R,R)-11 and (R,R)-12 in the range 220–400 nm.

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Figure 3: Minimized molecular structures of (from top left to bottom left, clockwise): (R,R)-10, (R,R)-11, (R,...

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Figure 4: Aromatic region of the ¹H NMR (CDCl₃, 500 MHz, 25 °C) spectra of macrocycle (R,R)-12 (2.8 mM, botto...

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Published 28 Jun 2012

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